Injected bone cements based on magnesium-substituted whitlockite, containing sodium carboxymethyl cellulose
https://doi.org/10.24930/1681-9004-2025-25-2-355-364
EDN: WIOQME
Abstract
Research subject. Calcium-magnesium phosphate powder and cement materials and cement fluid containing sodium carboxymethylcellulose (CMC).
Aim. To develop injectable bone cements based on soluble phases of calcium and magnesium phosphates for possible use in minimally invasive surgery.
Methods. Fritsch Analysis 22 laser particle analyser, Shimadzu XRD-6000 diffractometer, Tescan Vega II scanning electron microscope with an Oxford Instruments Inca X-Act energy dispersive analyser, Tristar 3000 particle analyser, Brookfield DV2T viscometer, Instron 5581 and Instron 3382 universal testing machines were used to characterise the materials.
Results. The introduction of CMC resulted in an increase in the viscosity and surface tension of the cement fluid, which resulted in an increase in the injectability and cohesion in aqueous media of the resulting cement materials. The effects of CMC introduction and mechanochemical activation on the phase composition, setting time, microstructure, cohesion, injectability and strength properties of the cement materials were determined.
Keywords
About the Authors
M. A. GoldbergRussian Federation
Margarita A. Goldberg
119334; 49 Leninsky av.; Moscow
P. A. Krokhicheva
Russian Federation
Polina A. Krokhicheva
119334; 49 Leninsky av.; Moscow
D. R. Khayrutdinova
Russian Federation
Dinara R. Khayrutdinova
119334; 49 Leninsky av.; Moscow
A. S. Fomin
Russian Federation
Aleksander S. Fomin
119334; 49 Leninsky av.; Moscow
A. V. Leonov
Russian Federation
Aleksander V. Leonov
119991; 1А Lenin Hills; Moscow
A. S. Baikin
Russian Federation
Aleksander S. Baikin
119334; 49 Leninsky av.; Moscow
O. S. Antonova
Russian Federation
Olga S. Antonova
119334; 49 Leninsky av.; Moscow
A. M. Sentsova
Russian Federation
Anita M. Sentsova
119334; 49 Leninsky av.; Moscow
N. O. Donskaya
Russian Federation
Nadezhda O. Donskaya
119334; 49 Leninsky av.; Moscow
S. M. Barinov
Russian Federation
Sergey M. Barinov
119334; 49 Leninsky av.; Moscow
V. S. Komlev
Russian Federation
Vladimir S. Komlev
119334; 49 Leninsky av.; Moscow
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Review
For citations:
Goldberg M.A., Krokhicheva P.A., Khayrutdinova D.R., Fomin A.S., Leonov A.V., Baikin A.S., Antonova O.S., Sentsova A.M., Donskaya N.O., Barinov S.M., Komlev V.S. Injected bone cements based on magnesium-substituted whitlockite, containing sodium carboxymethyl cellulose. LITHOSPHERE (Russia). 2025;25(2):355-364. (In Russ.) https://doi.org/10.24930/1681-9004-2025-25-2-355-364. EDN: WIOQME